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DETECTING LOW-LEVEL SYNTHESIS IMPURITIES IN MODIFIED PHOSPHOROTHIOATE OLIGONUCLEOTIDES USING LIQUID CHROMATOGRAPHY – HIGH RESOLUTION MASS SPECTROMETRY

An LC-MS method based on the use of high resolution Fourier transform ion cyclotron resonance mass spectrometry (FTIRCMS) for profiling oligonucleotides synthesis impurities is described. [Image: see text] Oligonucleotide phosphorothioatediesters (phosphorothioate oligonucleotides), in which one of...

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Detalhes bibliográficos
Main Authors: Nikcevic, Irena, Wyrzykiewicz, Tadeusz K., Limbach, Patrick A.
Formato: Artigo
Idioma:Inglês
Publicado em: 2011
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC3146765/
https://ncbi.nlm.nih.gov/pubmed/21811394
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.ijms.2010.06.001
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