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Efficient, Highly Stereoselective Synthesis of α-Keto-deoxy-D-glycero-D-galacto-nonulosonic Acid (KDN) Glycosides by Means of the 4,5-O-Carbonate Protecting Group

[Image: see text] A 1-adamantyl thioglycoside derivative of KDN, derived from N-acetylneuraminic acid, carrying a 3,4-O-carbonate protecting group is a highy efficient and α-selective KDN donor on activation with NIS and TfOH in dichloromethane and acetonitrile at −78 °C. Glycosylations conducted wi...

תיאור מלא

שמור ב:
מידע ביבליוגרפי
Main Authors: Crich, David, Navuluri, Chandrasekhar
פורמט: Artigo
שפה:Inglês
יצא לאור: 2010
נושאים:
גישה מקוונת:https://ncbi.nlm.nih.gov/pmc/articles/PMC3064762/
https://ncbi.nlm.nih.gov/pubmed/20333634
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.200907178
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