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Synthesis of a Water-Soluble 1,3-bis(diphenylene)-2-phenylallyl (BDPA) Radical

[Image: see text] The design and synthesis of a water-soluble 1,3-bis(diphenylene)-2-phenylallyl (BDPA) radical via the conjugate addition of a derivatized fluorene nucelophile is described. The compound is designed for use in dynamic nuclear polarization NMR. Its 9 GHz EPR spectrum in glycerol/wate...

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Bibliographic Details
Main Authors: Dane, Eric L., Swager, Timothy M.
Format: Artigo
Language:Inglês
Published: 2010
Subjects:
Online Access:https://ncbi.nlm.nih.gov/pmc/articles/PMC2882179/
https://ncbi.nlm.nih.gov/pubmed/20420445
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo100577g
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