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Application of the Chloro Ketal Claisen Reaction to the Total Synthesis of Squalene

A short, highly stereoselective (over 97%) synthesis of all-trans squalene is described. Starting with succinaldehyde, a tetraenedichlorodione having the complete squalene skeleton with the four internal trans olefinic bonds has been developed in four steps involving a sequence of two double Claisen...

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Bibliografiske detaljer
Udgivet i:Proc Natl Acad Sci U S A
Main Authors: Werthemann, Lucius, Johnson, William S.
Format: Artigo
Sprog:Inglês
Udgivet: National Academy of Sciences 1970
Fag:
Online adgang:https://ncbi.nlm.nih.govhttps://pmc.ncbi.nlm.nih.gov/articles/PMC283375/
https://ncbi.nlm.nih.govhttps://pubmed.ncbi.nlm.nih.gov/5274470/
https://ncbi.nlm.nih.govhttps://doi.org/10.1073/pnas.67.3.1465
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