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Heparan Sulfate Separation, Sequencing, and Isomeric Differentiation: Ion Mobility Spectrometry Reveals Specific Iduronic and Glucuronic Acid-Containing Hexasaccharides
We describe the resolution of heparan sulfate (HS) isomers by chromatographic methods and their subsequent differentiation by mass spectrometry (MS), ion mobility, and (1)H-NMR analysis. The two purified hexasaccharide isomers produced nearly identical MS spectra, quantitative disaccharide profiles,...
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| Main Authors: | , , , , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado: |
2009
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| Assuntos: | |
| Acceso en liña: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2810830/ https://ncbi.nlm.nih.gov/pubmed/19925012 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ac902186h |
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