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Synthesis of protected norcysteines for SPPS compatible with Fmoc-strategy
We report the synthesis of racemic Alloc-Ncy(Tmob)-OH, the resolution of its methyl ester, and demonstrate its application to form a norcystine bridge in octreotide-amide using the Fmoc-strategy on solid phase. N-Alloc and S-Tmob protections of norcysteine (Ncy) were found to be a preferred choice f...
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| Hoofdauteurs: | , |
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| Formaat: | Artigo |
| Taal: | Inglês |
| Gepubliceerd in: |
2007
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| Onderwerpen: | |
| Online toegang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2701708/ https://ncbi.nlm.nih.gov/pubmed/19562100 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2007.05.082 |
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