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Asymmetric synthesis of biaryl atropisomers by dynamic resolution on condensation of biaryl aldehydes with (−)-ephedrine or a proline-derived diamine

Atropisomeric biaryl aldehydes undergo diastereoselective condensation with (−)-ephedrine and with a proline-derived diamine, with selectivity highly dependent on solvent, temperature and reaction conditions. Levels of thermodynamic control up to 5:1 may be obtained by heating the diamine with the a...

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Detalhes bibliográficos
Main Authors: Bracegirdle, Ann, Clayden, Jonathan, Lai, Lai Wah
Formato: Artigo
Idioma:Inglês
Publicado em: Beilstein-Institut 2008
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC2633665/
https://ncbi.nlm.nih.gov/pubmed/19190743
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.4.47
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