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Synthesis of [(HIPTNCH(2)CH(2))(3)N]V Compounds (HIPT = 3,5-(2,4,6-i-Pr(3)C(6)H(2))(2)C(6)H(3)) and an Evaluation of Vanadium for the Reduction of Dinitrogen to Ammonia
Green [HIPTN(3)N]V(THF) ([HIPTN(3)N](3−) = [(HIPTNCH(2)CH(2))(3)N](3−) where HIPT = 3,5-(2,4,6-i-Pr(3)C(6)H(2))(2)C(6)H(3)) can be prepared in 70–80% yield through addition of H(3)[HIPTN(3)N] to VCl(3)(THF)(3) in THF followed by addition of LiN(SiMe(3))(2). From [HIPTN(3)N]V(THF) the following have...
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| Hauptverfasser: | , , , |
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| Format: | Artigo |
| Sprache: | Inglês |
| Veröffentlicht: |
2006
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| Schlagworte: | |
| Online Zugang: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2526228/ https://ncbi.nlm.nih.gov/pubmed/17083217 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ic061554r |
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