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An Operationally Simple and Efficient Work-up Procedure for TBAF-mediated Desilylation; Application to Halichondrin Synthesis
An operationally simple and efficient work-up method for TBAF-mediated TBS-deprotection has been developed. The procedure includes addition of a sulfonic acid resin and calcium carbonate, followed by filtration and evaporation. This method eliminates the tedious aqueous-phase extraction process to r...
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| Main Authors: | , |
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| Format: | Artigo |
| Jezik: | Inglês |
| Izdano: |
2007
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| Teme: | |
| Online dostop: | https://ncbi.nlm.nih.gov/pmc/articles/PMC2519602/ https://ncbi.nlm.nih.gov/pubmed/17286380 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ol063113h |
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