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Synthesis of N-Fmoc-(2S,3S,4R)-3,4-dimethylglutamine. An Application of Lanthanide-Catalyzed Transamidation
N-Fmoc-(2S,3S,4R)-3,4-dimethylglutamine (6) was synthesized from t-butyl N-Boc-(2S,3S,4R)-dimethylpyroglutamate (13). This synthesis involved selective deprotection of a Boc group from a lactam nitrogen in the presence of a t-butyl ester, Fmoc protection of the lactam, and a lanthanide-catalyzed tra...
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| Main Authors: | , |
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| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2005
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC1780274/ https://ncbi.nlm.nih.gov/pubmed/16050680 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jo050518r |
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