Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR

The absolute configuration of retroflexanone (1) and a closely related phlorogluinol (2) was established using the advanced Mosher method and by application of HPLC-NMR. HPLC-NMR permitted a small scale Mosher method analysis to be carried out on these unstable phloroglucinols.

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Autores principales: Caleb Singleton, Robert Brkljača, Sylvia Urban
Formato: Artigo
Lenguaje:Inglês
Publicado: MDPI AG 2018-06-01
Colección:Marine Drugs
Materias:
Mosher
retroflexanone
phloroglucinol
HPLC-NMR
secondary alcohol
Acceso en línea:http://www.mdpi.com/1660-3397/16/6/205
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