Absolute Configuration Determination of Retroflexanone Using the Advanced Mosher Method and Application of HPLC-NMR

The absolute configuration of retroflexanone (1) and a closely related phlorogluinol (2) was established using the advanced Mosher method and by application of HPLC-NMR. HPLC-NMR permitted a small scale Mosher method analysis to be carried out on these unstable phloroglucinols.

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Main Authors: Caleb Singleton, Robert Brkljača, Sylvia Urban
Formato: Artigo
Idioma:Inglês
Publicado em: MDPI AG 2018-06-01
Colecção:Marine Drugs
Assuntos:
Mosher
retroflexanone
phloroglucinol
HPLC-NMR
secondary alcohol
Acesso em linha:http://www.mdpi.com/1660-3397/16/6/205
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