Biradicals based on PROXYL containing building blocks for efficient dynamic nuclear polarization in biotolerant media

A versatile strategy for synthesizing tailored peptide based biradicals is presented. By labeling the protected amino acid hydroxyproline with PROXYL via the OH functionality and using this building block in solid phase peptide synthesis (SPPS), the obtained peptides become polarization agents for D...

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Autori principali:	Kevin Herr, Mark V. Höfler, Henrike Heise, Fabien Aussenac, Felix Kornemann, David Rosenberger, Martin Brodrecht, Marcos de Oliveira, Jr., Gerd Buntkowsky, Torsten Gutmann
Natura:	Artigo
Lingua:	Inglês
Pubblicazione:	Elsevier 2024-09-01
Serie:	Journal of Magnetic Resonance Open
Soggetti:	Biradicals Peptides Spin labeling Solid-state nmr Dynamic nuclear polarization
Accesso online:	http://www.sciencedirect.com/science/article/pii/S2666441024000074
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