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Chiral isothiourea-catalyzed kinetic resolution of 4-hydroxy[2.2]paracyclophane

We herein report a method for the kinetic resolution of racemic 4-hydroxy[2.2]paracyclophane by means of a chiral isothiourea-catalyzed acylation with isobutyric anhydride. This protocol allows for a reasonable synthetically useful s-factor of 20 and provides a novel entry to obtain this interesting...

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Detalhes bibliográficos
Publicado no:Beilstein J Org Chem
Main Authors: Weinzierl, David, Waser, Mario
Formato: Artigo
Idioma:Inglês
Publicado em: Beilstein-Institut 2021
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC8042488/
https://ncbi.nlm.nih.gov/pubmed/33889220
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.17.68
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