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Concise Synthesis of (+)-[(13)C(4)]-Anatoxin-a by Dynamic Kinetic Resolution of a Cyclic Iminium Ion

An asymmetric total synthesis of [(13)C(4)]-anatoxina ([(13)C(4)]-1) has been developed from commercially available ethyl [(13)C(4)]-acetoacetate ([(13)C(4)]-15). The unique requirements associated with isotope incorporation inspired a new, robust, and highly scalable route, providing access to 0.11...

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Detalhes bibliográficos
Publicado no:Angew Chem Int Ed Engl
Main Authors: Lacharity, Jacob J., Mailyan, Artur K., Chen, Karen Y., Zakarian, Armen
Formato: Artigo
Idioma:Inglês
Publicado em: 2020
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC7409530/
https://ncbi.nlm.nih.gov/pubmed/32304178
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.202004464
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