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Enantiospecific deoxyfluorination of cyclic α-OH-β-ketoesters†
We herein report the deoxyfluorination of cyclic α-hydroxy-β-ketoesters using diethylaminosulfur trifluoride (DAST). The reaction proceeds with excellent levels of stereospecificity, giving the configurationally inverted α-fluoro-β-ketoesters in high yields under operationally simple conditions.
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| Publicado no: | Org Biomol Chem |
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| Main Authors: | , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2021
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC7116657/ https://ncbi.nlm.nih.gov/pubmed/33211788 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/d0ob02152k |
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