A biradical-tagged phospholipid as a polarizing agent for solid-state MAS Dynamic Nuclear Polarization NMR of membrane proteins

A novel Dynamic Nuclear Polarization (DNP) NMR polarizing agent ToSMTSL-PTE representing a phospholipid with a biradical TOTAPOL tethered to the polar head group has been synthesized, characterized, and employed to enhance solid-state Nuclear Magnetic Resonance (SSNMR) signal of a lipid-reconstitute...

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Publicado no:Solid State Nucl Magn Reson
Main Authors: Good, Daryl B., Voinov, Maxim A., Bolton, David, Ward, Meaghan E., Sergeyev, Ivan V., Caporini, Marc, Scheffer, Peter, Lo, Andy, Rosay, Melanie, Marek, Antonin, Brown, Leonid S., Smirnov, Alex I., Ladizhansky, Vlad
Formato: Artigo
Idioma:Inglês
Publicado em: 2019
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Article
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6709687/
https://ncbi.nlm.nih.gov/pubmed/31029957
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.ssnmr.2019.04.003
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