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Efficient Dynamic Nuclear Polarization at 800 MHz / 527 GHz with Trityl-nitroxide Biradicals
Cross-effect (CE) dynamic nuclear polarization (DNP) is a rapidly developing technique that enhances the signal intensities in magic angle spinning (MAS) NMR spectra. We report CE DNP experiments at 211, 600 and 800 MHz using a new series of biradical polarizing agents referred to as TEMTriPols, in...
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Publicado no: | Angew Chem Int Ed Engl |
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Main Authors: | , , , , , , , , , |
Formato: | Artigo |
Idioma: | Inglês |
Publicado em: |
2015
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Assuntos: | |
Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5407364/ https://ncbi.nlm.nih.gov/pubmed/26268156 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201504292 |
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