Efficient Dynamic Nuclear Polarization at 800 MHz / 527 GHz with Trityl-nitroxide Biradicals

Cross-effect (CE) dynamic nuclear polarization (DNP) is a rapidly developing technique that enhances the signal intensities in magic angle spinning (MAS) NMR spectra. We report CE DNP experiments at 211, 600 and 800 MHz using a new series of biradical polarizing agents referred to as TEMTriPols, in...

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Detalhes bibliográficos
Publicado no:Angew Chem Int Ed Engl
Main Authors: Mathies, Guinevere, Caporini, Marc A., Michaelis, Vladimir K., Liu, Yangping, Hu, Kan-Nian, Mance, Deni, Zweier, Jay L., Rosay, Melanie, Baldus, Marc, Griffin, Robert G.
Formato: Artigo
Idioma:Inglês
Publicado em: 2015
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Article
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5407364/
https://ncbi.nlm.nih.gov/pubmed/26268156
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201504292
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