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Direct Dynamic Nuclear Polarization of (15)N and (13)C Spins at 14.1 T Using a Trityl Radical and Magic Angle Spinning
We investigate solid-state dynamic nuclear polarization of (13)C and (15)N nuclei using monoradical trityl OX063 as a polarizing agent in a magnetic field of 14.1 T with magic angle spinning at ~100 K. We monitored the field dependence of direct (13)C and (15)N polarization for frozen [(13)C, (15)N]...
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| Publicat a: | Solid State Nucl Magn Reson |
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| Autors principals: | , , , , , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
2019
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6604067/ https://ncbi.nlm.nih.gov/pubmed/31026722 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.ssnmr.2019.03.009 |
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