Direct Dynamic Nuclear Polarization of (15)N and (13)C Spins at 14.1 T Using a Trityl Radical and Magic Angle Spinning

We investigate solid-state dynamic nuclear polarization of (13)C and (15)N nuclei using monoradical trityl OX063 as a polarizing agent in a magnetic field of 14.1 T with magic angle spinning at ~100 K. We monitored the field dependence of direct (13)C and (15)N polarization for frozen [(13)C, (15)N]...

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Bibliografiska uppgifter
I publikationen:Solid State Nucl Magn Reson
Huvudupphovsmän: Wang, Xiaoling, Caulkins, Bethany G, Riviere, Gwladys, Mueller, Leonard J, Mentink-Vigier, Frederic, Long, Joanna R
Materialtyp: Artigo
Språk:Inglês
Publicerad: 2019
Ämnen:
Article
Länkar:https://ncbi.nlm.nih.gov/pmc/articles/PMC6604067/
https://ncbi.nlm.nih.gov/pubmed/31026722
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.ssnmr.2019.03.009
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