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Protecting groups in nucleoside syntheses. IV. 5′-Halogeno-5′-deoxy-2′, 3′-cyclic sulphite isomers in the preparation of 5′-halogeno-5′-deoxy nucleosides
Two isomeric 5′-halogeno-2′,3′-sulphites, epimeric at sulphur atom, are formed from ribonucleosides with thionyl chloride-hexamethylphosphoric triamide reagent. The formation of 5′-chloro-2′,3′-sulphites with cytidine (95%) and/or adenosine (94%) in acetonitrile supports a new proposal of the reacti...
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| Publicado no: | Nucleic Acids Res |
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| Main Authors: | , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Oxford University Press
1978
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6581306/ https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1093/nar/1.suppl_1.s125 |
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