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Large‐Scale Asymmetric Synthesis of Fmoc‐(S)‐2‐Amino‐6,6,6‐Trifluorohexanoic Acid
Here we report the first large‐scale synthesis of Fmoc‐(S)‐2‐amino‐6,6,6‐trifluorohexanoic acid via asymmetric alkylation of chiral Ni(II)‐complex of glycine Schiff base with CF(3)(CH(2))(3)I. The synthesis was performed on over 100 g scale and can be recommended as the most advanced procedure for r...
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| Yayımlandı: | ChemistryOpen |
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| Asıl Yazarlar: | , , , , , |
| Materyal Türü: | Artigo |
| Dil: | Inglês |
| Baskı/Yayın Bilgisi: |
John Wiley and Sons Inc.
2019
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| Konular: | |
| Online Erişim: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6554705/ https://ncbi.nlm.nih.gov/pubmed/31183311 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/open.201900131 |
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