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Large‐Scale Asymmetric Synthesis of Fmoc‐(S)‐2‐Amino‐6,6,6‐Trifluorohexanoic Acid
Here we report the first large‐scale synthesis of Fmoc‐(S)‐2‐amino‐6,6,6‐trifluorohexanoic acid via asymmetric alkylation of chiral Ni(II)‐complex of glycine Schiff base with CF(3)(CH(2))(3)I. The synthesis was performed on over 100 g scale and can be recommended as the most advanced procedure for r...
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| Publicat a: | ChemistryOpen |
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| Autors principals: | , , , , , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
John Wiley and Sons Inc.
2019
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6554705/ https://ncbi.nlm.nih.gov/pubmed/31183311 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/open.201900131 |
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