(19)F Dynamic Nuclear Polarization at Fast Magic Angle Spinning for NMR of HIV-1 Capsid Protein Assemblies

We report remarkably high, up to 100-fold, signal enhancements in (19)F dynamic nuclear polarization (DNP) magic angle spinning (MAS) spectra at 14.1 T on HIV-1 CA capsid protein assemblies. These enhancements correspond to absolute sensitivity ratios of 12–29 and are of similar magnitude as seen fo...

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發表在:J Am Chem Soc
Main Authors: Lu, Manman, Wang, Mingzhang, Sergeyev, Ivan V., Quinn, Caitlin M., Struppe, Jochem, Rosay, Melanie, Maas, Werner, Gronenborn, Angela M., Polenova, Tatyana
格式: Artigo
語言:Inglês
出版: 2019
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Article
在線閱讀:https://ncbi.nlm.nih.gov/pmc/articles/PMC6521953/
https://ncbi.nlm.nih.gov/pubmed/30871317
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.8b09216
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