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Two-step Synthesis of Solasodine Pivalate from Diosgenin Pivalate

A two-step synthesis of solasodine pivalate from diosgenin pivalate is described. The key transformation involves the reaction of diosgenin pivalate with benzyl carbamate (CbzNH(2)) promoted by TMSOTf. During the reaction the F-ring of the spiroketal moiety opens up with a simultaneous introduction...

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Detalhes bibliográficos
Publicado no:Molecules
Main Authors: Wojtkielewicz, Agnieszka, Kiełczewska, Urszula, Morzycki, Jacek W.
Formato: Artigo
Idioma:Inglês
Publicado em: MDPI 2019
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6471385/
https://ncbi.nlm.nih.gov/pubmed/30901960
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/molecules24061132
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