Inline Reaction Monitoring of Amine-Catalyzed Acetylation of Benzyl Alcohol Using a Microfluidic Stripline Nuclear Magnetic Resonance Setup

[Image: see text] We present an in-depth study of the acetylation of benzyl alcohol in the presence of N,N-diisopropylethylamine (DIPEA) by nuclear magnetic resonance (NMR) monitoring of the reaction from 1.5 s to several minutes. We have adapted the NMR setup to be compatible to microreactor techno...

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Pubblicato in:J Am Chem Soc
Autori principali: Oosthoek-de Vries, Anna Jo, Nieuwland, Pieter J., Bart, Jacob, Koch, Kaspar, Janssen, Johannes W. G., van Bentum, P. Jan M., Rutjes, Floris P. J. T., Gardeniers, Han J. G. E., Kentgens, Arno P. M.
Natura: Artigo
Lingua:Inglês
Pubblicazione: American Chemical Society 2019
Accesso online:https://ncbi.nlm.nih.gov/pmc/articles/PMC6449804/
https://ncbi.nlm.nih.gov/pubmed/30864795
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.9b00039
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