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Ag(I)–C–H Activation Enables Near-Room-Temperature Direct α-Arylation of Benzo[b]thiophenes

[Image: see text] The first example of near-room-temperature α-arylation of benzo[b]thiophenes is reported. The discovery rests on the observation of a switch in α-/β-regioselectivity at different loadings of Pd(2)(dba)(3)·CHCl(3) in the coupling between benzo[b]thiophene and 4-iodotoluene. We show...

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Detalhes bibliográficos
Publicado no:J Am Chem Soc
Main Authors: Colletto, Chiara, Panigrahi, Adyasha, Fernández-Casado, Jaime, Larrosa, Igor
Formato: Artigo
Idioma:Inglês
Publicado em: American Chemical Society 2018
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC6370252/
https://ncbi.nlm.nih.gov/pubmed/29983049
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.8b05361
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