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Efficient (15)N-(13)C Polarization Transfer by Third-Spin Assisted Pulsed Cross Polarization Magic-Angle-Spinning NMR for Protein Structure Determination
We introduce a pulsed third-spin assisted recoupling experiment that produces high-intensity long-range (15)N-(13)C cross peaks using low radiofrequency (rf) energy. This Proton-Enhanced Rotor-echo Short Pulse IRradiATION Cross Polarization ((PERSPIRATION)CP) pulse sequence operates with the same pr...
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| Publicado no: | J Phys Chem B |
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| Main Authors: | , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2018
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC6314680/ https://ncbi.nlm.nih.gov/pubmed/30106585 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.jpcb.8b06400 |
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