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(15)N-(15)N Proton Assisted Recoupling in Magic Angle Spinning NMR

We describe a new magic angle spinning (MAS) NMR experiment for obtaining (15)N-(15)N correlation spectra. The approach yields direct information about the secondary and tertiary structure of proteins, including identification of α-helical stretches and inter-strand connectivity in antiparallel β-sh...

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Autors principals: Lewandowski, Józef R., De Paëpe, Gaël, Eddy, Matthew T., Griffin, Robert G.
Format: Artigo
Idioma:Inglês
Publicat: 2009
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Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC2754755/
https://ncbi.nlm.nih.gov/pubmed/19334788
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/ja806578y
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