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A General and Simple Diastereoselective Reduction by l-Selectride: Efficient Synthesis of Protected (4S,5S)-Dihydroxy Amides

A general approach to (4S,5S)-4-benzyloxy-5-hydroxy-N-(4-methoxybenzyl) amides 10 based on a diastereoselective reduction of (5S,6RS)-6-alkyl-5-benzyloxy-6-hydroxy-2-piperidinones 6 and their tautomeric ring-opened keto amides 7 is described. The reduction with l-Selectride at -20 °C to room tempera...

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Publicat a:Molecules
Autors principals: Yin, Bo, Ye, Dong-Nai, Yu, Kai-Hui, Liu, Liang-Xian
Format: Artigo
Idioma:Inglês
Publicat: Molecular Diversity Preservation International 2010
Matèries:
Accés en línia:https://ncbi.nlm.nih.gov/pmc/articles/PMC6257261/
https://ncbi.nlm.nih.gov/pubmed/20428078
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3390/molecules15042771
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