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Syntheses of PDE3A inhibitor ORG9935 and determination of the absolute stereochemistries of its enantiomers by X-ray crystallography

Two synthetic methods were developed for the synthesis of PDE3A inhibitor ORG9935. The first one proceeds in six steps and 34% overall yield and the second one in five steps and an overall yield of 69% starting from commercially available starting material 5,6-dimethoxybenzo[b]thiophene-2-carboxylic...

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Bibliographic Details
Published in:Tetrahedron
Main Authors: Jakkaraj, Sudhakar, Young, Victor G., Georg, Gunda I.
Format: Artigo
Language:Inglês
Published: 2018
Subjects:
Online Access:https://ncbi.nlm.nih.gov/pmc/articles/PMC6223663/
https://ncbi.nlm.nih.gov/pubmed/30416214
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tet.2018.04.045
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