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NMR Signal Quenching from Bound Biradical Affinity Reagents in DNP Samples

We characterize the effect of specifically bound biradicals on the NMR spectra of dihydrofolate reductase from E. coli. Dynamic nuclear polarization methods enhance the signal-to-noise of solid state NMR experiments by transferring polarization from unpaired electrons of biradicals to nuclei. There...

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Detalhes bibliográficos
Publicado no:J Phys Chem B
Main Authors: Rogawski, Rivkah, Sergeyev, Ivan V., Zhang, Yinglu, Tran, Timothy H., Li, Yongjun, Tong, Liang, McDermott, Ann E.
Formato: Artigo
Idioma:Inglês
Publicado em: 2017
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Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5842680/
https://ncbi.nlm.nih.gov/pubmed/29116793
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.jpcb.7b08274
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