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Efficient assignment and NMR analysis of an intact virus using sequential side-chain correlations and DNP sensitization

An experimental strategy has been developed to increase the efficiency of dynamic nuclear polarization (DNP) in solid-state NMR studies. The method makes assignments simpler, faster, and more reliable via sequential correlations of both side-chain and Cα resonances. The approach is particularly suit...

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Bibliografski detalji
Izdano u:Proc Natl Acad Sci U S A
Glavni autori: Sergeyev, Ivan V., Itin, Boris, Rogawski, Rivkah, Day, Loren A., McDermott, Ann E.
Format: Artigo
Jezik:Inglês
Izdano: National Academy of Sciences 2017
Teme:
Online pristup:https://ncbi.nlm.nih.gov/pmc/articles/PMC5441803/
https://ncbi.nlm.nih.gov/pubmed/28461483
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1073/pnas.1701484114
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