Expanding the Horizons for Structural Analysis of Fully Protonated Protein Assemblies by NMR Spectroscopy at MAS Frequencies Above 100 kHz

The recent breakthroughs in NMR probe technologies resulted in the development of MAS NMR probes with rotation frequencies exceeding 100 kHz. Herein, we explore dramatic increases in sensitivity and resolution observed at MAS frequencies of 110–111 kHz in a novel 0.7 mm HCND probe that enable struct...

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Udgivet i:Solid State Nucl Magn Reson
Main Authors: Struppe, Jochem, Quinn, Caitlin M., Lu, Manman, Wang, Mingzhang, Hou, Guangjin, Lu, Xingyu, Kraus, Jodi, Andreas, Loren B., Stanek, Jan, Lalli, Daniela, Lesage, Anne, Pintacuda, Guido, Maas, Werner, Gronenborn, Angela M., Polenova, Tatyana
Format: Artigo
Sprog:Inglês
Udgivet: 2017
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Article
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC5824719/
https://ncbi.nlm.nih.gov/pubmed/28732673
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.ssnmr.2017.07.001
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