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Quantification of 3-ketodihydrosphingosine using HPLC-ESI-MS/MS to study SPT activity in yeast Saccharomyces cerevisiae

Serine palmitoyltransferase (SPT) catalyzes the rate-limiting step of condensation of L-serine and palmitoyl-CoA to form 3-ketodihydrosphingosine (3KDS). Here, we report a HPLC-ESI-MS/MS method to directly quantify 3KDS generated by SPT. With this technique, we were able to detect 3KDS at a level co...

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Detalhes bibliográficos
Publicado no:J Lipid Res
Main Authors: Ren, Jihui, Snider, Justin, Airola, Michael V., Zhong, Aaron, Rana, Nadia A., Obeid, Lina M., Hannun, Yusuf A.
Formato: Artigo
Idioma:Inglês
Publicado em: The American Society for Biochemistry and Molecular Biology 2018
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5748491/
https://ncbi.nlm.nih.gov/pubmed/29092960
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1194/jlr.D078535
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