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Enhancing the Sensitivity of Multidimensional NMR Experiments by using Triply-Compensated π Pulses
In multidimensional solution NMR experiments, π pulses are used extensively for inversion and refocusing operations on (1)H, (13)C and (15)N nuclei. Pulse miscalibration, off-resonance effects, and J-coupling evolution during π pulse execution result in severe signal losses that are exacerbated at h...
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| Yayımlandı: | J Biomol NMR |
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| Asıl Yazarlar: | , , , , , , , |
| Materyal Türü: | Artigo |
| Dil: | Inglês |
| Baskı/Yayın Bilgisi: |
2017
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| Konular: | |
| Online Erişim: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5738291/ https://ncbi.nlm.nih.gov/pubmed/29164453 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-017-0153-2 |
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