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(15)N and (13)C-SOFAST-HMQC editing enhances 3D-NOESY sensitivity in highly deuterated, selectively [(1)H,(13)C]-labeled proteins
The ongoing NMR method development effort strives for high quality multidimensional data with reduced collection time. Here, we apply ‘SOFAST-HMQC’ to frequency editing in 3D HMQC-NOESY-HMQC and demonstrate the sensitivity benefits using highly deuterated and (15)N, methyl labeled samples in H(2)O....
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| Publicado no: | J Biomol NMR |
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| Main Authors: | , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5218894/ https://ncbi.nlm.nih.gov/pubmed/27878649 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1007/s10858-016-0074-5 |
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