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Synthesis of a 1,3-Bridged Macrobicyclic Enyne via Chemoselective Cycloisomerization Using Palladium-catalyzed Alkyne-Alkyne Coupling
A unique intramolecular Pd-catalyzed alkyne-alkyne coupling is presented. This transformation generates a strained, 1,3-bridged, macrocyclic enyne. The process was readily executed on gram-scale, and the structure of the product was elucidated via X-ray crystallographic analysis. A mechanistic ratio...
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| Izdano u: | J Org Chem |
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| Glavni autori: | , , , |
| Format: | Artigo |
| Jezik: | Inglês |
| Izdano: |
2016
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| Teme: | |
| Online pristup: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5726859/ https://ncbi.nlm.nih.gov/pubmed/27648602 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.6b01920 |
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