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Removal of Triphenylphosphine Oxide by Precipitation with Zinc Chloride in Polar Solvents

[Image: see text] While the use of triphenylphosphine as a reductant is common in organic synthesis, the resulting triphenylphosphine oxide (TPPO) waste can be difficult to separate from the reaction product. While a number of strategies to precipitate TPPO are available, none have been reported to...

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Detalhes bibliográficos
Publicado no:J Org Chem
Main Authors: Batesky, Donald C., Goldfogel, Matthew J., Weix, Daniel J.
Formato: Artigo
Idioma:Inglês
Publicado em: American Chemical Society 2017
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5634519/
https://ncbi.nlm.nih.gov/pubmed/28956444
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.7b00459
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