Automated Synthesis of 1-[(11)C]acetoacetate on a TRASIS AIO module

We automated radiochemical synthesis of 1-[(11)C]acetoacetate in a commercially available radiochemistry module, TRASIS AllInOne by [(11)C]carboxylation of the corresponding enolate anion generated in situ from isopropenylacetate and MeLi, and purified by ion-exchange column resins.1-[(11)C]acetoace...

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Publicado en:Appl Radiat Isot
Main Authors: Sai, Kiran Kumar Solingapuram, Gage, H. Donald, Almaguel, Frankis, Neth, Bryan, Hughes, Timothy M., Tremblay, Sebastien, Castellano, Christian-Alexandre, Cunnane, Stephen C., Jorgensen, Matthew J., Craft, Suzanne, Mintz, Akiva
Formato: Artigo
Idioma:Inglês
Publicado: 2017
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Article
Acceso en liña:https://ncbi.nlm.nih.gov/pmc/articles/PMC5612895/
https://ncbi.nlm.nih.gov/pubmed/28806598
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.apradiso.2017.07.066
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