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Stereoselective Synthesis of the Equatorial Glycosides of Legionaminic Acid
The synthesis of a legionaminic acid donor from N-acetyl neuraminic acid in fifteen steps and 17% overall yield is described. Activation of the adamantanyl thioglycoside in the donor with N-iodosuccinimide and trifluoromethanesulfonic acid in dichloromethane and acetonitrile at −78 °C in the presenc...
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| Publicat a: | J Org Chem |
|---|---|
| Autors principals: | , , |
| Format: | Artigo |
| Idioma: | Inglês |
| Publicat: |
2017
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| Matèries: | |
| Accés en línia: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5545936/ https://ncbi.nlm.nih.gov/pubmed/28530837 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.7b00746 |
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