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Stereoselective Synthesis of the Equatorial Glycosides of Legionaminic Acid
The synthesis of a legionaminic acid donor from N-acetyl neuraminic acid in fifteen steps and 17% overall yield is described. Activation of the adamantanyl thioglycoside in the donor with N-iodosuccinimide and trifluoromethanesulfonic acid in dichloromethane and acetonitrile at −78 °C in the presenc...
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| Vydáno v: | J Org Chem |
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| Hlavní autoři: | , , |
| Médium: | Artigo |
| Jazyk: | Inglês |
| Vydáno: |
2017
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| Témata: | |
| On-line přístup: | https://ncbi.nlm.nih.gov/pmc/articles/PMC5545936/ https://ncbi.nlm.nih.gov/pubmed/28530837 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.7b00746 |
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