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Syntheses of (+)-30-epi-, (−)-6-epi-, (±)-6,30-epi-13,14-Didehydroxyisogarcinol and (±)-6,30-epi-Garcimultiflorone A Utilizing Highly Diastereoselective, Lewis Acid-Controlled Cyclizations

The first syntheses of 13,14-didehydroxyisogarcinol (6) and garcimultiflorone A (5) stereoisomers are reported in six steps from a commercially available phloroglucinol. Lewis acid-controlled, diastereoselective cationic oxycyclizations enabled asymmetric syntheses of (−)-6-epi-6 and (+)-30-epi-6. A...

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Detalhes bibliográficos
Publicado no:J Am Chem Soc
Main Authors: Boyce, Jonathan H., Eschenbrenner-Lux, Vincent, Porco, John A.
Formato: Artigo
Idioma:Inglês
Publicado em: 2016
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC5315221/
https://ncbi.nlm.nih.gov/pubmed/27744695
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/jacs.6b09727
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