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TMSBr-mediated solvent- and work-up-free synthesis of α-2-deoxyglycosides from glycals
The thio-additions of glycals were efficiently promoted by a stoichiometric amount of trimethylsilyl bromide (TMSBr) to produce S-2-deoxyglycosides under solvent-free conditions in good to excellent yields. In addition, with triphenylphosphine oxide as an additive, the TMSBr-mediated direct glycosyl...
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| Publicado no: | Beilstein J Org Chem |
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| Main Authors: | , , , , |
| Formato: | Artigo |
| Idioma: | Inglês |
| Publicado em: |
Beilstein-Institut
2016
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| Assuntos: | |
| Acesso em linha: | https://ncbi.nlm.nih.gov/pmc/articles/PMC4979735/ https://ncbi.nlm.nih.gov/pubmed/27559420 https://ncbi.nlm.nih.govhttp://dx.doi.org/10.3762/bjoc.12.164 |
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