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Stereoselective Synthesis of Trisubstituted Vinyl Bromides by Addition of Alkynes to Oxocarbenium Ions

We have developed an efficient method for the synthesis of (E)-trisubstituted vinyl bromides via a Friedel–Crafts-type addition of alkynes to oxocarbenium ions formed in situ from acetals. The success of this reaction relies on identification of MgBr(2)·OEt(2) as both a Lewis acid promoter and bromi...

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Detalhes bibliográficos
Publicado no:Synlett
Main Authors: Ehle, Andrew R., Morris, Melissa G., Klebon, Bryan D., Yap, Glenn P. A., Watson, Mary P.
Formato: Artigo
Idioma:Inglês
Publicado em: 2015
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4961304/
https://ncbi.nlm.nih.gov/pubmed/27482143
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1055/s-0035-1560265
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