Efficient Synthesis of Molecular Precursors for Parahydrogen-Induced Polarization of Ethyl Acetate-1-(13)C and Beyond

Scalable and versatile methodology for production of vinylated carboxylic compounds with (13)C isotopic label in C1 position is described. It afforded robust synthesis of vinyl acetate-1-(13)C, which is a precursor for preparation of (13)C hyperpolarized ethyl acetate-1-(13)C, which provides a conve...

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Vydáno v:Angew Chem Int Ed Engl
Hlavní autoři: Shchepin, Roman V., Barskiy, Danila A., Coffey, Aaron M., Manzanera Esteve, Isaac V., Chekmenev, Eduard Y.
Médium: Artigo
Jazyk:Inglês
Vydáno: 2016
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On-line přístup:https://ncbi.nlm.nih.gov/pmc/articles/PMC4939483/
https://ncbi.nlm.nih.gov/pubmed/27061815
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201600521
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