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Optimising selective excitation pulses to maximise saturation transfer difference NMR spectroscopy

A simple method is presented that optimizes the STD NMR Gaussian pulse to deliver significant increases in STD amplification factors with minimal perturbation of the ligand. This approach is practically demonstrated using the wheat-germ agglutinin/N-acetyl-D-glucosamine protein-ligand system.

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Bibliografiska uppgifter
I publikationen:RSC Adv
Huvudupphovsmän: Ley, Nathan B., Rowe, Michelle L., Williamson, Richard A., Howard, Mark J.
Materialtyp: Artigo
Språk:Inglês
Publicerad: 2014
Ämnen:
Länkar:https://ncbi.nlm.nih.gov/pmc/articles/PMC4864509/
https://ncbi.nlm.nih.gov/pubmed/27182436
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/C3RA46246C
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