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Optimising selective excitation pulses to maximise saturation transfer difference NMR spectroscopy

A simple method is presented that optimizes the STD NMR Gaussian pulse to deliver significant increases in STD amplification factors with minimal perturbation of the ligand. This approach is practically demonstrated using the wheat-germ agglutinin/N-acetyl-D-glucosamine protein-ligand system.

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Detalhes bibliográficos
Publicado no:RSC Adv
Main Authors: Ley, Nathan B., Rowe, Michelle L., Williamson, Richard A., Howard, Mark J.
Formato: Artigo
Idioma:Inglês
Publicado em: 2014
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4864509/
https://ncbi.nlm.nih.gov/pubmed/27182436
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1039/C3RA46246C
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