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A Single-Flask Synthesis of α-Alkylidene and α-Benzylidene Lactones from Ethoxyacetylene, Epoxides/Oxetanes, and Carbonyl Compounds

Low temperature treatment of (ethoxyethynyl)lithium with epoxides or oxetanes in the presence of BF(3)•OEt(2), followed by addition of aldehydes or ketones and warming to room temperature, affords structurally diverse five- and six-membered α-alkylidene and α-benzylidene lactones (5) in good to exce...

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Detalhes bibliográficos
Publicado no:Tetrahedron Lett
Main Authors: Ng, Kevin, Tran, Vincent, Minehan, Thomas
Formato: Artigo
Idioma:Inglês
Publicado em: 2016
Assuntos:
Acesso em linha:https://ncbi.nlm.nih.gov/pmc/articles/PMC4698893/
https://ncbi.nlm.nih.gov/pubmed/26744547
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1016/j.tetlet.2015.12.041
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