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Palladium-Catalyzed Decarbonylative Dehydration for the Synthesis of α-Vinyl Carbonyl Compounds and Total Synthesis of (−)-Aspewentin A, B, and C

The direct α-vinylation of carbonyl compounds that forms a quaternary stereocenter is a challenging transformation. We discovered that δ-oxocarboxylic acids can serve as masked vinyl compounds and be unveiled by palladium-catalyzed decarbonylative dehydration. The carboxylic acids are readily availa...

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Pubblicato in:Angew Chem Int Ed Engl
Autori principali: Liu, Yiyang, Virgil, Scott C., Grubbs, Robert H., Stoltz, Brian M.
Natura: Artigo
Lingua:Inglês
Pubblicazione: 2015
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Accesso online:https://ncbi.nlm.nih.gov/pmc/articles/PMC4686263/
https://ncbi.nlm.nih.gov/pubmed/26230413
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1002/anie.201505161
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