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Synthesis of (±)-Tetrabenazine by Visible Light Photoredox Catalysis

(±)-Tetrabenazine was synthesized in six steps from commercially available compounds. The key cyclization substrate was assembled rapidly via Baylis-Hillman and aza-Michael reactions. Annulation of the final ring was achieved through visible light photocatalysis, wherein carbon-carbon bond formation...

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Bibliografiske detaljer
Udgivet i:J Org Chem
Main Authors: Orgren, Lindsey R., Maverick, Emily E., Marvin, Christopher C.
Format: Artigo
Sprog:Inglês
Udgivet: 2015
Fag:
Online adgang:https://ncbi.nlm.nih.gov/pmc/articles/PMC4684717/
https://ncbi.nlm.nih.gov/pubmed/26544155
https://ncbi.nlm.nih.govhttp://dx.doi.org/10.1021/acs.joc.5b02199
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